8EOZ
Precisely patterned nanofibers made from extendable protein multiplexes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-29 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97 |
Spacegroup name | H 3 |
Unit cell lengths | 68.225, 68.225, 139.038 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 46.350 - 3.000 |
R-factor | 0.2371 |
Rwork | 0.232 |
R-free | 0.28670 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Designed Model |
RMSD bond length | 0.002 |
RMSD bond angle | 0.435 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.350 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Rmerge | 0.040 | |
Number of reflections | 4528 | 328 |
<I/σ(I)> | 10.95 | 4.09 |
Completeness [%] | 93.5 | 99.9 |
Redundancy | 1.3 | 1 |
CC(1/2) | 0.990 | 0.850 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Imidazole.HCl pH 8.0 15% (w/v) MPD; 5% (w/v) PEG 4000 |