8ECV
Bovine Fab 2F12
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-1 |
Synchrotron site | SSRL |
Beamline | BL12-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-22 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.366, 73.735, 142.831 |
Unit cell angles | 90.00, 91.96, 90.00 |
Refinement procedure
Resolution | 36.980 - 1.810 |
R-factor | 0.2213 |
Rwork | 0.219 |
R-free | 0.26120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6oo0 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.722 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.000 | 1.830 |
High resolution limit [Å] | 1.810 | 1.810 |
Rmerge | 0.136 | 0.934 |
Rmeas | 0.166 | 1.130 |
Rpim | 0.093 | 0.634 |
Number of reflections | 70456 | 3942 |
<I/σ(I)> | 10.1 | 2 |
Completeness [%] | 88.1 | 97.8 |
Redundancy | 2.9 | 3 |
CC(1/2) | 0.951 | 0.401 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.2 | 293.15 | 0.2M sodium chloride, 0.1M phosphate-citrate buffer, 20% Peg6000 |