8D8G
Crystal structure of hen egg white lysozyme at 325 Kelvin (Duplicate)
Experimental procedure
Experimental method | LAUE |
Source type | ROTATING ANODE |
Source details | BRUKER TURBO X-RAY SOURCE |
Temperature [K] | 325 |
Detector technology | CMOS |
Collection date | 2020-11-24 |
Detector | BRUKER PHOTON 100 |
Wavelength(s) | 1.54184 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.814, 79.814, 37.713 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.719 - 1.500 |
Rwork | 0.200 |
R-free | 0.23650 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a8z |
RMSD bond length | 0.011 |
RMSD bond angle | 1.650 |
Data reduction software | SAINT |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.720 | 35.720 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 19859 | 18782 |
<I/σ(I)> | 5.33 | |
Completeness [%] | 97.5 | |
Redundancy | 1.8 | |
CC(1/2) | 0.535 | 0.535 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295 | 1.2 M NaCl and 100 mM AcONa pH 4.6 |