8D8D
Crystal structure of hen egg white lysozyme at 300 Kelvin (Duplicate)
Experimental procedure
Experimental method | LAUE |
Source type | ROTATING ANODE |
Source details | BRUKER TURBO X-RAY SOURCE |
Temperature [K] | 300 |
Detector technology | CMOS |
Collection date | 2020-11-24 |
Detector | BRUKER PHOTON 100 |
Wavelength(s) | 1.54184 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.484, 79.484, 37.860 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.575 - 1.500 |
Rwork | 0.176 |
R-free | 0.20300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a8z |
RMSD bond length | 0.013 |
RMSD bond angle | 1.833 |
Data reduction software | SAINT |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.580 | 22.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 19919 | 18893 |
<I/σ(I)> | 10.61 | |
Completeness [%] | 99.5 | |
Redundancy | 1.9 | |
CC(1/2) | 0.736 | 0.736 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295 | 1.2 M NaCl and 100 mM AcONa pH 4.6 |