8CJW

Nucleoprotein Thogotovirus delta188-196

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-10-16
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9814, 0.97973
Spacegroup name	H 3
Unit cell lengths	119.110, 119.110, 91.638
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	41.874 - 2.010
R-factor	0.187
Rwork	0.185
R-free	0.23390
Structure solution method	SAD
RMSD bond length	0.008
RMSD bond angle	0.896
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHELX
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.900	2.130
High resolution limit [Å]	2.010	2.010
Rmeas	0.056	0.198
Number of reflections	32179	5199
<I/σ(I)>	15.3
Completeness [%]	99.5	99.1
Redundancy	4.3	4.2
CC(1/2)	0.995	0.329

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	293	21% PEG 1500, 0.1M SPG pH 7.0