8CIH
Structure of FL CINP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-11-26 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 61 |
| Unit cell lengths | 91.722, 91.722, 134.368 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 51.300 - 2.000 |
| R-factor | 0.2115 |
| Rwork | 0.210 |
| R-free | 0.23130 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.391 |
| Data reduction software | autoPROC |
| Data scaling software | STARANISO |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 51.300 | 2.100 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.122 | |
| Rmeas | 0.127 | |
| Rpim | 0.035 | |
| Number of reflections | 43390 | 40485 |
| <I/σ(I)> | 14.4 | |
| Completeness [%] | 95.7 | 93.8 |
| Redundancy | 13.3 | |
| CC(1/2) | 0.900 | 0.700 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6.2 | 292.15 | 25% (v/v) 1,2-propanediol, 10% (v/v) glycerol and 100 mM sodium potassium phosphate pH 6.2 |
