8CGT

STRUCTURE OF CYCLODEXTRIN GLYCOSYLTRANSFERASE COMPLEXED WITH A THIO-MALTOHEXAOSE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	298
Detector technology	AREA DETECTOR
Collection date	1996-11-01
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	94.400, 104.900, 113.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.400
R-factor	0.157
Rwork	0.157
R-free	0.17800
Structure solution method	OTHER
RMSD bond length	0.010
RMSD bond angle	1.300
Data reduction software	XDS
Data scaling software	XDS
Refinement software	X-PLOR (3.851)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	34.317	2.260
High resolution limit [Å]	2.200	2.200
Number of reflections	48544
<I/σ(I)>	15.1	4.3
Completeness [%]	84.2	51.9
Redundancy	3.2	1.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.9		pH 6.9