8C0L
FC-THF stabilizer of 14-3-3 and ERalpha
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-09 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.033200 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 81.880, 112.141, 62.707 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.070 - 1.600 |
R-factor | 0.1832 |
Rwork | 0.182 |
R-free | 0.20760 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.062 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2-4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.130 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 38541 | 1854 |
<I/σ(I)> | 17 | |
Completeness [%] | 99.9 | |
Redundancy | 12.9 | |
CC(1/2) | 0.989 | 0.862 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.095 M HEPES (pH 7.1), PEG400 (24% (v/v)), 0.19 M CaCl2 and 5% (v/v) Glycerol |