8BYW

Rut B structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-03-15
Detector	DECTRIS PILATUS 300K
Wavelength(s)	1.0
Spacegroup name	P 1
Unit cell lengths	69.562, 108.252, 123.744
Unit cell angles	85.74, 83.33, 74.27

Refinement procedure

Resolution	48.710 - 1.590
R-factor	0.2075
Rwork	0.206
R-free	0.23290
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.852
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.18rc2)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.710	1.647
High resolution limit [Å]	1.590	1.590
Number of reflections	447821	43730
<I/σ(I)>	7.55
Completeness [%]	96.5
Redundancy	3.5
CC(1/2)	0.995	0.481

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	PEG