8BXT
Structure of StayGold
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-07-20 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.95373 |
| Spacegroup name | P 61 |
| Unit cell lengths | 133.721, 133.721, 58.533 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 66.660 - 1.600 |
| Rwork | 0.163 |
| R-free | 0.18460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.520 |
| Data reduction software | DIALS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 66.660 | 1.630 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rpim | 0.062 | 0.555 |
| Number of reflections | 78841 | 3870 |
| <I/σ(I)> | 9.1 | 1.6 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 20.5 | 20.8 |
| CC(1/2) | 0.998 | 0.695 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 290 | PEG |
