8BKN
Carboxymyoglobin dark state for comparison with 5 mJ/cm2 time series
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | OTHER |
| Temperature [K] | 293 |
| Detector technology | PIXEL |
| Collection date | 2019-05-01 |
| Detector | CUSTOM-MADE |
| Wavelength(s) | 1.03 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 63.000, 28.400, 35.300 |
| Unit cell angles | 90.00, 107.00, 90.00 |
Refinement procedure
| Resolution | 30.120 - 1.290 |
| R-factor | 0.1779 |
| Rwork | 0.175 |
| R-free | 0.21010 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5d5r |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.024 |
| Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.120 | 1.320 |
| High resolution limit [Å] | 1.290 | 1.290 |
| Number of reflections | 30443 | 1976 |
| <I/σ(I)> | 5.7 | |
| Completeness [%] | 99.9 | |
| Redundancy | 264.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | 3.1 M ammonium sulfate |
