8BKD
structure of RutB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-07-18 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 122.920, 111.610, 128.980 |
| Unit cell angles | 90.00, 99.14, 90.00 |
Refinement procedure
| Resolution | 48.220 - 1.400 |
| R-factor | 0.1688 |
| Rwork | 0.169 |
| R-free | 0.21240 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.792 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXCD |
| Refinement software | PHENIX (1.18rc2) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.220 | 1.450 |
| High resolution limit [Å] | 1.400 | 1.400 |
| Number of reflections | 661819 | 64589 |
| <I/σ(I)> | 11.03 | |
| Completeness [%] | 98.3 | |
| Redundancy | 11.1 | |
| CC(1/2) | 0.990 | 0.400 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG |
