8AXR

Crystal structure of the C-terminal domain of human CFAP410

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-2
Synchrotron site	ESRF
Beamline	ID23-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-03-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.87313
Spacegroup name	C 1 2 1
Unit cell lengths	56.115, 50.628, 22.146
Unit cell angles	90.00, 101.08, 90.00

Refinement procedure

Resolution	19.940 - 1.500
R-factor	0.2139
Rwork	0.211
R-free	0.24190
Structure solution method	AB INITIO PHASING
RMSD bond length	0.006
RMSD bond angle	0.937
Data reduction software	xia2
Data scaling software	xia2
Phasing software	Arcimboldo
Refinement software	PHENIX (1.19.1_4122)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.940	1.550
High resolution limit [Å]	1.500	1.500
Rmerge	0.077
Rmeas	0.084
Rpim	0.034
Number of reflections	9761	948
<I/σ(I)>	11.05
Completeness [%]	99.6
Redundancy	6.2
CC(1/2)	0.999	0.519

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		297	1.5 M sodium chloride, 10% (v/v) ethanol