8AW8
Xylose Isomerase in 70% relative humidity environment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2022-02-16 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 82.826, 96.307, 97.757 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.830 - 1.630 |
R-factor | 0.1615 |
Rwork | 0.160 |
R-free | 0.19370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6rnf |
RMSD bond length | 0.008 |
RMSD bond angle | 1.054 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.830 | 1.690 |
High resolution limit [Å] | 1.630 | 1.630 |
Rmerge | 0.088 | 1.600 |
Number of reflections | 60298 | 3015 |
<I/σ(I)> | 11.9 | |
Completeness [%] | 61.9 | |
Redundancy | 6.2 | |
CC(1/2) | 0.999 | 0.593 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | 35% (w/v) PEG3350, 200 mM lithium sulfate and 10 mM Hepes/NaOH, pH 7.5 |