8ARL

Plasmodium vivax PVP01_0000100 TRAg domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-08-07
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97950
Spacegroup name	P 21 21 21
Unit cell lengths	49.200, 52.362, 102.554
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.630 - 1.450
R-factor	0.2265
Rwork	0.225
R-free	0.25320
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	RobettaFold model
RMSD bond length	0.003
RMSD bond angle	0.525
Data reduction software	DIALS
Data scaling software	DIALS
Phasing software	PHASER
Refinement software	PHENIX (1.16_3549)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.360	1.470
High resolution limit [Å]	1.450	1.450
Number of reflections	47846	2325
<I/σ(I)>	12.8
Completeness [%]	100.0
Redundancy	6.6
CC(1/2)	0.999	0.497

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	SPG pH 4.0, PEG1500