Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-09-30 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 44.450, 48.150, 73.750 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 32.682 - 1.500 |
| Rwork | 0.155 |
| R-free | 0.17460 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 3dkx |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.905 |
| Data reduction software | MOSFLM |
| Data scaling software | pointless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 32.660 | 32.660 |
| High resolution limit [Å] | 1.500 | 1.500 |
| Rmerge | 0.186 | 1.387 |
| Rpim | 0.023 | |
| Number of reflections | 26009 | 1268 |
| <I/σ(I)> | 9.1 | |
| Completeness [%] | 99.8 | |
| Redundancy | 13.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.1 M Tri-sodium citrate pH 5.0 1M LiCl 30 % PEG 6000 |
