Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-04-15 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 60.462, 155.959, 141.322 |
| Unit cell angles | 90.00, 92.64, 90.00 |
Refinement procedure
| Resolution | 48.784 - 2.006 |
| Rwork | 0.180 |
| R-free | 0.23200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4mj1 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.714 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.082 |
| High resolution limit [Å] | 2.006 | 2.006 |
| Number of reflections | 164438 | 17100 |
| <I/σ(I)> | 8.35 | |
| Completeness [%] | 94.8 | |
| Redundancy | 6.6 | |
| CC(1/2) | 0.994 | 0.852 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293.15 | PEG 3.350 Lithium Chloride HEPES |
