8A8Y
Structure of truncated 1-deoxy-D-xylulose 5-phosphate synthase (DXS) from Klebsiella pneumoniae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-04-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 119.164, 144.247, 142.911 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.935 - 2.100 |
R-factor | 0.18023954443 |
Rwork | 0.179 |
R-free | 0.20105 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2o1s |
RMSD bond length | 0.002 |
RMSD bond angle | 0.527 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 91.900 | 2.210 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.089 | 0.720 |
Number of reflections | 71565 | 10344 |
<I/σ(I)> | 9.9 | |
Completeness [%] | 99.6 | |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG 8000, Magnesium chloride, TRIS |