7ZHC
Moss spermine/spermidine acetyl transferase (PpSSAT) in complex with AcetylCoA and polyethylen glycol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-05-26 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99187 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.108, 97.773, 48.453 |
Unit cell angles | 90.00, 117.40, 90.00 |
Refinement procedure
Resolution | 48.890 - 1.819 |
R-factor | 0.2015 |
Rwork | 0.199 |
R-free | 0.23400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bei |
RMSD bond length | 0.008 |
RMSD bond angle | 0.940 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3 (18-SEP-2020)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.890 | 2.050 |
High resolution limit [Å] | 1.819 | 1.819 |
Rmerge | 0.102 | 1.138 |
Number of reflections | 23866 | 1194 |
<I/σ(I)> | 9.3 | |
Completeness [%] | 92.1 | |
Redundancy | 6.4 | |
CC(1/2) | 0.998 | 0.497 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292 | 10% PEG 8000, 10% PEG 1000 |