Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-01-29 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 1 |
| Unit cell lengths | 49.710, 53.820, 60.480 |
| Unit cell angles | 90.11, 96.98, 94.66 |
Refinement procedure
| Resolution | 40.577 - 1.560 |
| Rwork | 0.176 |
| R-free | 0.20900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5dyv |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.666 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.580 | 40.540 |
| High resolution limit [Å] | 1.560 | 1.560 |
| Rmeas | 0.033 | 0.047 |
| Number of reflections | 84307 | 84307 |
| <I/σ(I)> | 11.3 | 11.3 |
| Completeness [%] | 95.5 | |
| Redundancy | 3.5 | |
| CC(1/2) | 1.000 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.25 M Magnesium Chloride 0.1M HEPES 10% PEG 6K |
