7Z6F
Crystal structure of the substrate-binding protein YejA in complex with peptide fragment
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-10-13 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.531, 76.972, 103.817 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 62.190 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.116 | 1.355 |
Number of reflections | 68508 | 3281 |
<I/σ(I)> | 7.4 | 1 |
Completeness [%] | 99.6 | 95.9 |
Redundancy | 4.3 | |
CC(1/2) | 0.995 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 293 | 25% PEG 3350, 0.1 M Bis-Tris pH 5.5 |