7YUJ

Crystal structure of HOIL-1L(365-510)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-07-04
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.97918
Spacegroup name	P 1 21 1
Unit cell lengths	53.252, 59.870, 57.818
Unit cell angles	90.00, 90.92, 90.00

Refinement procedure

Resolution	26.623 - 1.865
R-factor	0.1547
Rwork	0.153
R-free	0.18680
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	57.810	1.970
High resolution limit [Å]	1.865	1.870
Rmerge	0.087	0.390
Number of reflections	27779	2558
<I/σ(I)>	12
Completeness [%]	91.4
Redundancy	5.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		289	22 % w/v Poly(acrylic acid sodium salt) 5,100, 100 mM HEPES(pH 7.5), 20 mM Magnesium chloride