7YT9

crystal structure of AGD1-4 of Arabidopsis AGDP3

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-12-13
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9789
Spacegroup name	I 21 21 21
Unit cell lengths	78.538, 129.205, 167.049
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	47.810 - 2.600
R-factor	0.2461
Rwork	0.245
R-free	0.27220
Structure solution method	SAD
Data reduction software	HKL-3000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	50.000	50.000	2.690
High resolution limit [Å]	2.600	5.600	2.600
Rmerge	0.039	0.024	0.705
Rmeas	0.045	0.028	0.798
Rpim	0.021	0.013	0.368
Total number of observations	116578
Number of reflections	26390	2751	2611
<I/σ(I)>	10.6
Completeness [%]	99.2	98.1	99.7
Redundancy	4.4	4.3	4.5
CC(1/2)		0.999	0.834

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5.5	293	0.1 M lithium sulfate, 20% PEG1000 and 0.1M sodium citrate, pH 5.5