7YRA
Crystal structure of [2Fe-2S]-TtPetA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 15 |
| Detector technology | PIXEL |
| Collection date | 2020-11-24 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 32.409, 51.022, 98.805 |
| Unit cell angles | 90.00, 93.45, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.790 |
| Rwork | 0.207 |
| R-free | 0.23860 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7yr9 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.900 |
| High resolution limit [Å] | 1.790 | 1.790 |
| Number of reflections | 30162 | 4797 |
| <I/σ(I)> | 10.1 | |
| Completeness [%] | 99.4 | |
| Redundancy | 3.4 | |
| CC(1/2) | 0.995 | 0.927 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.6 M AmS, 20% glycerol, 0.1 M Na-Ac pH 4.6 |
