Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-1A |
| Synchrotron site | Photon Factory |
| Beamline | BL-1A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-05-05 |
| Detector | DECTRIS EIGER X 4M |
| Wavelength(s) | 1.1 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 177.380, 47.760, 81.780 |
| Unit cell angles | 90.00, 97.93, 90.00 |
Refinement procedure
| Resolution | 46.090 - 2.200 |
| R-factor | 0.2429 |
| Rwork | 0.242 |
| R-free | 0.26710 |
| Structure solution method | SAD |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.602 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (v1.0) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.090 | 2.279 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.064 | 1.265 |
| Rmeas | 0.071 | 0.071 |
| Rpim | 0.030 | 0.577 |
| Number of reflections | 34504 | 3381 |
| <I/σ(I)> | 15.03 | 1.33 |
| Completeness [%] | 98.7 | 97.77 |
| Redundancy | 5.2 | 5.5 |
| CC(1/2) | 0.999 | 0.819 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 290 | 0.2 M Ammonium Sulfate 0.1 M MES:NaOH pH 6.5 30% (w/v) PEG 5000 MME |
