7YEJ
TR-SFX MmCPDII-DNA complex: 100 ns time-point collected in SACLA. Includes 100 ns, dark, and extrapolated structure factors
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | SACLA BEAMLINE BL2 |
Synchrotron site | SACLA |
Beamline | BL2 |
Temperature [K] | 298 |
Detector technology | CCD |
Collection date | 2019-05-28 |
Detector | MPCCD |
Wavelength(s) | 1.0875 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 72.530, 115.710, 169.280 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.050 - 2.550 |
R-factor | 0.2039 |
Rwork | 0.203 |
R-free | 0.22350 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7ydz |
RMSD bond length | 0.004 |
RMSD bond angle | 0.529 |
Data reduction software | CrystFEL |
Data scaling software | pointless |
Phasing software | REFMAC |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.050 | 2.570 |
High resolution limit [Å] | 2.550 | 2.550 |
Number of reflections | 47318 | 2372 |
<I/σ(I)> | 8.74 | 2.84 |
Completeness [%] | 100.0 | 100 |
Redundancy | 361.07 | 207.3 |
CC(1/2) | 0.987 | 0.836 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 4.6 | 296 | 100 mM Sodium Acetate pH 4.6 250 mM ammonium sulfate 4% PEG4000 (w/v) 50 mM DTT |