7YC6
Crystal structure of D110P mutant of GATase subunit of Methanocaldococcus jannaschii GMP synthetase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 277 |
Detector technology | IMAGE PLATE |
Collection date | 2022-03-22 |
Detector | MAR scanner 345 mm plate |
Wavelength(s) | 1.54179 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 63.080, 63.080, 101.940 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 54.630 - 2.400 |
R-factor | 0.19987 |
Rwork | 0.199 |
R-free | 0.22123 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7d40 |
RMSD bond length | 0.011 |
RMSD bond angle | 1.594 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.630 | 2.530 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.160 | |
Number of reflections | 9659 | 9659 |
<I/σ(I)> | 16.1 | |
Completeness [%] | 100.0 | |
Redundancy | 12.8 | |
CC(1/2) | 0.995 | 0.995 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICROBATCH | 298 | 0.2M Zinc acetate dihydrate, 20% PEG 3350, pH 6.4 |