7Y8W
Crystal structure of DLC-1/SAO-1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-10-20 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.98 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 40.274, 163.515, 229.132 |
Unit cell angles | 90.00, 90.46, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.400 |
R-factor | 0.2544 |
Rwork | 0.253 |
R-free | 0.28490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3p8m |
RMSD bond length | 0.003 |
RMSD bond angle | 0.707 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.440 |
High resolution limit [Å] | 2.400 | 6.510 | 2.400 |
Rmerge | 0.129 | 0.058 | 0.762 |
Rmeas | 0.142 | 0.064 | 0.847 |
Rpim | 0.059 | 0.026 | 0.361 |
Total number of observations | 285979 | ||
Number of reflections | 55428 | 2653 | 2782 |
<I/σ(I)> | 3.9 | ||
Completeness [%] | 95.3 | 89.7 | 97 |
Redundancy | 5.2 | 5.2 | 4.9 |
CC(1/2) | 0.996 | 0.775 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.2 M Potassium chloride, 0.05 M HEPES pH 7.5, 35% (v/v) Pentaerythritol propoxylate |