7Y6Y

RLGSGG-AtPRT6 UBR box (C121)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	193
Detector technology	PIXEL
Collection date	2019-11-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	60.706, 87.128, 60.777
Unit cell angles	90.00, 98.43, 90.00

Refinement procedure

Resolution	24.740 - 1.543
R-factor	0.2271
Rwork	0.226
R-free	0.24270
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6lhn
RMSD bond length	0.010
RMSD bond angle	1.060
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	24.740	1.598
High resolution limit [Å]	1.543	1.543
Number of reflections	45502	4463
<I/σ(I)>	31.675
Completeness [%]	96.7
Redundancy	4.1
CC(1/2)	0.995	0.946

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	0.2 M Calcium acetate hydrate, 20% (w/v) PEG 3350