7Y6X

RRGSGG-AtPRT6 UBR box (P32)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 11C
Synchrotron site	PAL/PLS
Beamline	11C
Temperature [K]	193
Detector technology	PIXEL
Collection date	2019-12-14
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 32
Unit cell lengths	93.670, 93.670, 106.970
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.650 - 2.196
R-factor	0.2014
Rwork	0.201
R-free	0.22020
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6lhn
RMSD bond length	0.013
RMSD bond angle	1.142
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.650	2.275
High resolution limit [Å]	2.196	2.196
Number of reflections	52178	4996
<I/σ(I)>	10.73077
Completeness [%]	97.1
Redundancy	5.5
CC(1/2)	0.976	0.390

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	295	1.2 M DL-Malic acid pH 7.0, 0.1 M BIS-Tris pH 7.0