7XYI
HapR Quadruple mutant Y76F, L97I, I141V, F171C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER X8 PROTEUM |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-23 |
Detector | Bruker PHOTON III |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 88.545, 43.448, 53.499 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.750 - 2.470 |
R-factor | 0.2158 |
Rwork | 0.211 |
R-free | 0.25550 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 7xxo |
Data reduction software | PROTEUM PLUS |
Data scaling software | PROTEUM PLUS |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.830 | 2.560 |
High resolution limit [Å] | 2.470 | 2.470 |
Number of reflections | 14299 | 774 |
<I/σ(I)> | 12.5 | 2.5 |
Completeness [%] | 99.9 | |
Redundancy | 8.6 | |
CC(1/2) | 0.998 | 0.700 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 9.5 | 297 | 8%PEG 8000, 100mM CHES 9.5, 200mM NaCl |