Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-11-01 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97915 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 93.765, 93.765, 150.344 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.600 - 2.950 |
| Rwork | 0.305 |
| R-free | 0.32370 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1i78 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.743 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (V1.6) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.890 | 3.130 |
| High resolution limit [Å] | 2.950 | 2.950 |
| Rmeas | 0.170 | |
| Rpim | 0.038 | 0.634 |
| Number of reflections | 16591 | 2635 |
| <I/σ(I)> | 13.4 | |
| Completeness [%] | 99.6 | |
| Redundancy | 19.8 | |
| CC(1/2) | 0.999 | 0.586 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | MPD |
