7XSF
Crystal structure of ClAgl29A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 74.577, 95.521, 83.550 |
Unit cell angles | 90.00, 97.33, 90.00 |
Refinement procedure
Resolution | 47.806 - 2.006 |
Rwork | 0.205 |
R-free | 0.24270 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xsd |
RMSD bond length | 0.004 |
RMSD bond angle | 1.082 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0349) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 82.900 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmeas | 0.090 | 0.960 |
Number of reflections | 76908 | 12196 |
<I/σ(I)> | 14.8 | 2.45 |
Completeness [%] | 98.9 | 97.3 |
Redundancy | 7 | |
CC(1/2) | 0.999 | 0.900 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M sodium citrate (pH 5.5), 16% PEG3,350 |