7XSF
Crystal structure of ClAgl29A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-09-12 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 74.577, 95.521, 83.550 |
| Unit cell angles | 90.00, 97.33, 90.00 |
Refinement procedure
| Resolution | 47.806 - 2.006 |
| Rwork | 0.205 |
| R-free | 0.24270 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2xsd |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.082 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | REFMAC (5.8.0349) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 82.900 | 2.100 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmeas | 0.090 | 0.960 |
| Number of reflections | 76908 | 12196 |
| <I/σ(I)> | 14.8 | 2.45 |
| Completeness [%] | 98.9 | 97.3 |
| Redundancy | 7 | |
| CC(1/2) | 0.999 | 0.900 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M sodium citrate (pH 5.5), 16% PEG3,350 |
