7XQS

The structure of FLA-K*00701/KP-CoV-9

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-07-21
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97918
Spacegroup name	P 21 21 21
Unit cell lengths	54.292, 70.829, 121.347
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.890 - 2.690
R-factor	0.2259
Rwork	0.223
R-free	0.29210
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5xmf
RMSD bond length	0.009
RMSD bond angle	1.171
Phasing software	PHASER
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	61.170	2.830
High resolution limit [Å]	2.690	2.690
Rmerge	0.074	0.857
Number of reflections	13627	13627
<I/σ(I)>	22
Completeness [%]	99.2
Redundancy	12.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	291.15	0.1M Sodium chloride, 0.1M HEPES PH 7, 25% (W/V) SOKALAN PA 25 CL