Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NFPSS BEAMLINE BL19U1 |
| Synchrotron site | NFPSS |
| Beamline | BL19U1 |
| Temperature [K] | 233 |
| Detector technology | CCD |
| Collection date | 2018-06-19 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9793 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 71.762, 82.426, 104.839 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 54.124 - 1.781 |
| R-factor | 0.2086 |
| Rwork | 0.208 |
| R-free | 0.22370 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7wx6 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.177 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 54.124 | 1.810 |
| High resolution limit [Å] | 1.781 | 1.781 |
| Number of reflections | 29485 | 29485 |
| <I/σ(I)> | 8.7 | |
| Completeness [%] | 99.9 | |
| Redundancy | 11.9 | |
| CC(1/2) | 0.927 | 0.927 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | PEG3350,BIS-TRIS5.5 |
