7WAW

MurJ inward closed form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL32XU
Synchrotron site	SPring-8
Beamline	BL32XU
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-10-09
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.9794
Spacegroup name	P 1 21 1
Unit cell lengths	56.410, 71.460, 74.540
Unit cell angles	90.00, 96.98, 90.00

Refinement procedure

Resolution	44.070 - 2.800
R-factor	0.2221
Rwork	0.216
R-free	0.27260
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	1.032
Refinement software	PHENIX ((1.18.2_3874: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.070	2.900
High resolution limit [Å]	2.800	2.800
Number of reflections	14632	1450
<I/σ(I)>	3.75
Completeness [%]	100.0
Redundancy	12.3
CC(1/2)	0.944	0.684

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIPIDIC CUBIC PHASE		293.15	MPD, MgCl2, Tris-HCl