Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2017-05-29 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.97732 |
| Spacegroup name | P 1 |
| Unit cell lengths | 81.854, 92.301, 109.894 |
| Unit cell angles | 77.47, 70.69, 64.36 |
Refinement procedure
| Resolution | 44.997 - 2.671 |
| R-factor | 0.2375 |
| Rwork | 0.236 |
| R-free | 0.26770 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4plc |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.461 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.997 | 2.671 |
| High resolution limit [Å] | 2.671 | 2.671 |
| Rmerge | 0.078 | 0.503 |
| Number of reflections | 72344 | 72344 |
| <I/σ(I)> | 1.81 | |
| Completeness [%] | 93.5 | |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293.15 | 1M Lithium Chloride, 0.1M Sodium Acetate and 25-30% (w/v) PEG 6000 |
