7W1R
Crystal structure of human Suv3 monomer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-16 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9 |
Spacegroup name | P 32 |
Unit cell lengths | 92.409, 92.409, 88.057 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 36.430 - 3.200 |
R-factor | 0.2445 |
Rwork | 0.240 |
R-free | 0.28640 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rc3 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.764 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.310 |
High resolution limit [Å] | 3.200 | 3.200 |
Number of reflections | 13937 | 1079 |
<I/σ(I)> | 33.1 | |
Completeness [%] | 95.8 | |
Redundancy | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.005 M Magnesium sulfate heptahydrate, 0.05 M MES monohydrate pH 6.0, 5% w/v PEG 4000 |