7W1C
Crystal structure of Klebsiella pneumoniae K1 capsule-specific polysaccharide lyase in a P1 crystal form
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL15A1 |
Synchrotron site | NSRRC |
Beamline | BL15A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-10-27 |
Detector | RAYONIX MX300HE |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
Unit cell lengths | 90.281, 100.574, 125.033 |
Unit cell angles | 80.50, 70.32, 83.43 |
Refinement procedure
Resolution | 30.000 - 1.480 |
R-factor | 0.139 |
Rwork | 0.137 |
R-free | 0.18400 |
Structure solution method | MAD |
RMSD bond length | 0.018 |
RMSD bond angle | 1.697 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELX |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 1.530 |
High resolution limit [Å] | 1.480 | 1.480 |
Rmerge | 0.073 | 0.741 |
Number of reflections | 656693 | 64500 |
<I/σ(I)> | 25.44 | 2.28 |
Completeness [%] | 97.0 | 95.4 |
Redundancy | 3.7 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 15% (W/V) PEG 4000, 0.2 M IMIDAZOLE MALATE, PH 6.0, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 293K |