Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 78 |
| Detector technology | PIXEL |
| Collection date | 2021-06-20 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.987 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 100.665, 126.842, 144.993 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.550 - 1.590 |
| R-factor | 0.1689 |
| Rwork | 0.168 |
| R-free | 0.19260 |
| Structure solution method | SAD |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.730 | 1.680 |
| High resolution limit [Å] | 1.586 | 1.590 |
| Number of reflections | 249003 | 39127 |
| <I/σ(I)> | 15.1 | |
| Completeness [%] | 99.6 | |
| Redundancy | 13 | |
| CC(1/2) | 0.999 | 0.770 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION, RECRYSTALLIZATION | 6 | 277 | 0.2M Ammonium sulfate, 20% w/v polyethylene glycol 3350 |
