7VT2

Azumapecten Farreri ferritin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-05-23
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9789
Spacegroup name	P 1 2 1
Unit cell lengths	161.535, 169.579, 198.374
Unit cell angles	90.00, 95.73, 90.00

Refinement procedure

Resolution	29.680 - 2.400
R-factor	0.1904
Rwork	0.190
R-free	0.23020
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6a4u
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.680	2.490
High resolution limit [Å]	2.160	2.400
Rmerge	0.162
Rpim	0.103
Number of reflections	4102168	552777
<I/σ(I)>	4.8
Completeness [%]	98.1
Redundancy	3.4
CC(1/2)		0.985

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG3350, succinic acid, pH7.0