7VSS

Phosphoglucomutase_tlr1976

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-11-02
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97915
Spacegroup name	P 41 21 2
Unit cell lengths	110.082, 110.082, 177.645
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.730 - 2.960
R-factor	0.1911
Rwork	0.188
R-free	0.22780
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1kfq
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.740	3.140
High resolution limit [Å]	2.960	2.960
Rmerge	0.062	0.519
Number of reflections	23412	3703
<I/σ(I)>	29
Completeness [%]	99.7
Redundancy	12.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	NaCl