Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-07-13 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 129.310, 168.473, 41.492 |
| Unit cell angles | 90.00, 90.06, 90.00 |
Refinement procedure
| Resolution | 38.480 - 2.790 |
| R-factor | 0.1916 |
| Rwork | 0.190 |
| R-free | 0.21850 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 7CQ9 |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.548 |
| Data reduction software | HKL-3000 (v705c) |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.900 |
| High resolution limit [Å] | 2.790 | 2.800 |
| Rmerge | 0.060 | |
| Number of reflections | 21080 | 1712 |
| <I/σ(I)> | 16.91 | |
| Completeness [%] | 95.6 | |
| Redundancy | 3.4 | |
| CC(1/2) | 0.918 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 8 | 293 | 0.1M Tris pH 8.0, 1.6M Li2SO4 |
