7VCM

crystal structure of GINKO1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-08-23
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 1
Unit cell lengths	46.827, 49.319, 83.683
Unit cell angles	89.96, 89.97, 80.95

Refinement procedure

Resolution	42.080 - 1.850
Rwork	0.195
R-free	0.22520
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6gel 5FIM
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	MOLREP
Refinement software	PHENIX (1.19)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.107	1.920
High resolution limit [Å]	1.850	1.850
Number of reflections	56403	5152
<I/σ(I)>	6.3
Completeness [%]	93.5
Redundancy	1.9
CC(1/2)	0.993	0.591

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1M MES pH 6.0, 20% PEG6000