7TFY

[T:Ag+/Hg2+:T--(pH11-pH7; 300s)] Metal-mediated DNA base pair in tensegrity triangle grown at pH 11 and soaked in pH 7 for 300s

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-11-14
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00743
Spacegroup name	H 3
Unit cell lengths	106.187, 106.187, 89.408
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	32.400 - 4.710
R-factor	0.2591
Rwork	0.256
R-free	0.32640
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	0.980
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	AutoSol
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	64.100	5.430
High resolution limit [Å]	4.710	4.710
Number of reflections	2660	382
<I/σ(I)>	9.8
Completeness [%]	84.4
Redundancy	10.5
CC(1/2)	0.998	0.445

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	11	293	Tris, magnesium sulfate, silver nitrate, mercury chloride