Experimental procedure
| Source type | ELECTRON MICROSCOPE |
| Collection date | 2018-10-17 |
| Wavelength(s) | 0.0251 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 4.830, 23.100, 29.840 |
| Unit cell angles | 90.00, 92.00, 90.00 |
Refinement procedure
| Resolution | 18.262 - 1.050 |
| Rwork | 0.181 |
| R-free | 0.20100 |
| RMSD bond length | 0.015 |
| RMSD bond angle | 1.843 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 18.262 | 18.262 | 1.080 |
| High resolution limit [Å] | 1.050 | 4.700 | 1.050 |
| Rmerge | 0.156 | 0.147 | 0.712 |
| Rmeas | 0.161 | 0.151 | 0.776 |
| Total number of observations | 36014 | ||
| Number of reflections | 2596 | 20 | 153 |
| <I/σ(I)> | 8.24 | 14.48 | 1.79 |
| Completeness [%] | 83.3 | 64.5 | 69.9 |
| Redundancy | 13.873 | 10.7 | 7.196 |
| CC(1/2) | 0.994 | 0.993 | 0.572 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
