7SLO

[U:Ag+:U--pH 11] Metal-mediated DNA base pair in tensegrity triangle

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-07-18
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00743
Spacegroup name	H 3
Unit cell lengths	106.636, 106.636, 91.897
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	41.260 - 4.120
R-factor	0.2597
Rwork	0.259
R-free	0.26340
Structure solution method	SAD
RMSD bond length	0.012
RMSD bond angle	1.417
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	AutoSol
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	65.140	4.610
High resolution limit [Å]	4.120	4.120
Number of reflections	1925	192
<I/σ(I)>	6.7
Completeness [%]	79.4
Redundancy	3.8
CC(1/2)	0.992	0.232

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	11	293	Tris, Magnesium sulfate, silver nitrate