7SLC

[T:Ag+:T--pH 9] Metal-mediated DNA base pair in tensegrity triangle

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-10-17
Detector	DECTRIS EIGER2 X 9M
Wavelength(s)	1.00743
Spacegroup name	H 3
Unit cell lengths	105.497, 105.497, 92.758
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	32.550 - 4.020
R-factor	0.2482
Rwork	0.246
R-free	0.28090
Structure solution method	SAD
RMSD bond length	0.015
RMSD bond angle	1.546
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	AutoSol
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	65.090	4.420
High resolution limit [Å]	4.020	4.020
Number of reflections	2236	207
<I/σ(I)>	8.8
Completeness [%]	87.1
Redundancy	10.2
CC(1/2)	0.999	0.021

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	293	Tris, Magnesium sulfate, silver nitrate