7RXU
Crystal structure of Cj1090c
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-11-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9788 |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 89.071, 89.071, 118.220 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 14.940 - 2.400 |
R-factor | 0.2006 |
Rwork | 0.199 |
R-free | 0.23680 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 0.575 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | SOLVE |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 | 2.400 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.051 | 0.290 |
Number of reflections | 11050 | 11050 |
<I/σ(I)> | 14.4 | |
Completeness [%] | 97.4 | |
Redundancy | 14.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 290 | PEG 8000, calcium acetate, glycerol, MES |