7RXI

Fab234 in complex with the C-terminal alpha-TSR domain of P. falciparum

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL12-2
Synchrotron site	SSRL
Beamline	BL12-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-11-11
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.97946
Spacegroup name	P 41 21 2
Unit cell lengths	115.690, 115.690, 119.297
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.080 - 2.150
R-factor	0.2211
Rwork	0.219
R-free	0.26470
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	Homology model
RMSD bond length	0.012
RMSD bond angle	1.037
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	PHASER
Refinement software	PHENIX ((1.19_4092: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.190
High resolution limit [Å]	2.150	2.150
Rpim	0.042	0.458
Number of reflections	43634	2124
<I/σ(I)>	21.2	1.8
Completeness [%]	97.9	97.2
Redundancy	5.5	4.6
CC(1/2)	0.928	0.730

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	293.15	20% PEG8000, 0.1 M HEPES, pH 7.5